Modern Supercritical Fluid Chromatography

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  • Publisher : John Wiley & Sons
  • Release : 05 November 2019
  • ISBN : 9781119625995
  • Page : 416 pages
  • Rating : 4.5/5 from 103 voters

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Explains why modern supercritical fluid chromatography (SFC) is the leading "green" analytical and purification separations technology. Modern supercritical fluid chromatography (SFC) is the leading method used to analyze and purify chiral and achiral chemical compounds, many of which are pharmaceuticals, pharmaceutical candidates, and natural products including cannabis-related compounds. This book covers current SFC instrumentation as it relates to greater robustness, better reproducibility, and increased analytical sensitivity. Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases covers the history, instrumentation, method development and applications of SFC. The authors provided readers with an overview of analytical and preparative SFC equipment, stationary phases, and mobile phase choices. Topics covered include: Milestones of Supercritical Fluid Chromatography; Physical Properties of Supercritical Fluids; Instrumentation for SFC; Detection in SFC; Achiral SFC Method Development; Chiral SFC Method Development; and Preparative Scale SFC. The book also includes highlights of modern applications of SFC in the final chapters—namely pharmaceuticals, consumer products, foods, polymers, petroleum-related mixtures, and cannabis—and discusses the future of SFC. Provides a clear explanation of the physical and chemical properties of supercritical fluids, which gives the reader a better understanding of the basis for improved performance in SFC compared to HPLC and GC Describes the advantages of SFC as a green alternative to HPLC and GC for the analysis of both polar, water-soluble, and non-polar analytes Details both achiral and chiral SFC method development, including modifiers, additives, the impact of temperature and pressure, and stationary phase choices Details why SFC is the premier modern preparative chromatographic technique used to purify components of mixtures for subsequent uses, both from performance and economic perspectives Covers numerous detectors, with an emphasis on SFC-MS, SFC-UV, and SFC-ELSD (evaporative light scattering detection) Describes the application of SFC to numerous high-value application areas Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases will be of great interest to professionals, students, and professors involved in analytical, bioanalytical, separations science, medicinal, petroleum, and environmental chemistries. It will also appeal to pharmaceutical scientists, natural-product scientists, food and consumer-products scientists, chemical engineers, and managers in these areas.

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Modern Supercritical Fluid Chromatography

Modern Supercritical Fluid Chromatography
  • Author : Larry M. Miller,J. David Pinkston,Larry T. Taylor
  • Publisher : John Wiley & Sons
  • Release Date : 2019-11-05
  • ISBN : 9781119625995
GET THIS BOOKModern Supercritical Fluid Chromatography

Explains why modern supercritical fluid chromatography (SFC) is the leading "green" analytical and purification separations technology. Modern supercritical fluid chromatography (SFC) is the leading method used to analyze and purify chiral and achiral chemical compounds, many of which are pharmaceuticals, pharmaceutical candidates, and natural products including cannabis-related compounds. This book covers current SFC instrumentation as it relates to greater robustness, better reproducibility, and increased analytical sensitivity. Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases covers the history, instrumentation, method

Practical Supercritical Fluid Chromatography and Extraction

Practical Supercritical Fluid Chromatography and Extraction
  • Author : Thomas Caudell
  • Publisher : Routledge
  • Release Date : 2018-05-08
  • ISBN : 9781351422512
GET THIS BOOKPractical Supercritical Fluid Chromatography and Extraction

An exploration of fundamental as well as practical aspects of supercritical fluid chromatography and extraction. It addresses topics such as: packed columns in SFC; detection in SFC; supercritical fluid chromatography/mass spectroscopy; and evaporative light scattering detection in SFC.

Analysis with Supercritical Fluids: Extraction and Chromatography

Analysis with Supercritical Fluids: Extraction and Chromatography
  • Author : Bernd Wenclawiak
  • Publisher : Springer Science & Business Media
  • Release Date : 2012-12-06
  • ISBN : 9783642774744
GET THIS BOOKAnalysis with Supercritical Fluids: Extraction and Chromatography

The use of supercritical fluids in analytical chemistry is still grow ing. More and more analysts are discovering the favorable advan tages for a number of applications. Especially supercritical fluid extraction (SFE) has attracted a lot of interest in recent years due to its simplicity. Supercritical fluid chromatography (SFC) has become better established and the development of this technique has been accelerated by the many applications with capillary col umns which have been published in the literature. At first SFC

Supercritical Fluid Chromatography

Supercritical Fluid Chromatography
  • Author : Gregory K. Webster
  • Publisher : CRC Press
  • Release Date : 2014-02-04
  • ISBN : 9789814463003
GET THIS BOOKSupercritical Fluid Chromatography

Analytical chemists in the pharmaceutical industry are always looking for more-efficient techniques to meet the analytical challenges of today’s pharmaceutical industry. One technique that has made steady advances in pharmaceutical analysis is supercritical fluid chromatography (SFC). SFC is meeting the chromatography needs of the industry by providing efficient and selective testing capabilities on the analytical and preparative scale. The supercritical fluid mobile phase, consisting mainly of CO2, facilitates cost reduction costs and helps the industry in meeting green chemistry

Supercritical Fluid Chromatography

Supercritical Fluid Chromatography
  • Author : Gérard Rossé
  • Publisher : Walter de Gruyter GmbH & Co KG
  • Release Date : 2018-12-17
  • ISBN : 9783110500776
GET THIS BOOKSupercritical Fluid Chromatography

Supercritical Fluid Chromatography (SFC) provides a timely overview of SFC application areas which were unimaginable just a decade ago. This two-volume series opens with an overview of the history and expectant future of SFC and continues with recent applications in the pharmaceutical industry and other fascinating areas of science. SFC has found its place in the pharmaceutical industry with an increasing body of applications for chiral and achiral molecules in both the research and development phases of the drug discovery

Supercritical Fluid Extraction and its Use in Chromatographic Sample Preparation

Supercritical Fluid Extraction and its Use in Chromatographic Sample Preparation
  • Author : S.A. Westwood
  • Publisher : Springer Science & Business Media
  • Release Date : 2012-12-06
  • ISBN : 9789401121644
GET THIS BOOKSupercritical Fluid Extraction and its Use in Chromatographic Sample Preparation

by Professor D. E. Games, Mass Spectrometry Research Unit, University College of Swansea Sample preparation can be viewed as occupying a Cinderella role in analytical science. However, the quality of sample preparation plays a key role in high In the past decade, there has been quality analysis and deserves higher stature. considerable interest in the use of supercritical fluid extraction (SFE) as an alternative to conventional procedures for the preparation of samples for ana lysis. The driving force for this

Packed Column SFC

Packed Column SFC
  • Author : T A Berger
  • Publisher : Royal Society of Chemistry
  • Release Date : 2007-10-31
  • ISBN : 9781847551603
GET THIS BOOKPacked Column SFC

Packed Column SFC is the third title to be published in this series and has been produced as a result of the dramatic re-emergence, in the last three years, of packed column instrumentation. This has led to a redefinition of the technique and an urgent need for a practical guide that deals with its subtleties. This book fulfils that need and deals exclusively with packed column SFC. It places the emphasis on understanding the underlying chemistry in order to perform

Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring

Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring
  • Author : Melissa N. Dunkle,William L. Winniford
  • Publisher : John Wiley & Sons
  • Release Date : 2020-09-01
  • ISBN : 9781119523307
GET THIS BOOKAnalytical Techniques in the Oil and Gas Industry for Environmental Monitoring

A thorough introduction to environmental monitoring in the oil and gas industry Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring examines the analytical side of the oil and gas industry as it also provides an overall introduction to the industry. You’ll discover how oil and natural gas are sourced, refined, and processed. You can learn about what’s produced from oil and natural gas, and why evaluating these sourced resources is important. The book discusses the

Supercritical Fluids

Supercritical Fluids
  • Author : E. Kiran,Pablo G. Debenedetti,Cor J. Peters
  • Publisher : Springer Science & Business Media
  • Release Date : 2012-12-06
  • ISBN : 9789401139298
GET THIS BOOKSupercritical Fluids

Supercritical fluids are neither gas nor liquid, but can be compressed gradually from low to high density and they are therefore interesting and important as tunable solvents and reaction media in the chemical process industry. By adjusting the density the properties of these fluids can be customised and manipulated for a given process - physical or chemical transformation. Separation and processing using supercritical solvents such as CO2 are currently on-line commercially in the food, essential oils and polymer industries. Many

Microbore Column Chromatography

Microbore Column Chromatography
  • Author : F. J. Yang
  • Publisher : CRC Press
  • Release Date : 2020-08-27
  • ISBN : 9781000147254
GET THIS BOOKMicrobore Column Chromatography

This book describes the various aspects of microbore column chromatography. It provides readers with an in-depth understanding of the supercritical fluid chromatography and microbore high-performance liquid chromatography.

Gradient HPLC for Practitioners

Gradient HPLC for Practitioners
  • Author : Stavros Kromidas
  • Publisher : John Wiley & Sons
  • Release Date : 2019-04-16
  • ISBN : 9783527812769
GET THIS BOOKGradient HPLC for Practitioners

This practical guide for analytical scientists explains the use of gradients in liquid chromatography. The fundamentals of gradient separations, as well as the most common application scenarios are addressed, from LC-MS coupling to biochromatography to the separation of ionic substances. Throughout, this handy volume provides detailed hands-on information for practitioners, enabling them to use gradient separation methods reliably and efficiently.

Applications of Supercritical Fluids in Industrial Analysis

Applications of Supercritical Fluids in Industrial Analysis
  • Author : J.R. Dean
  • Publisher : Springer Science & Business Media
  • Release Date : 2012-12-06
  • ISBN : 9789401121460
GET THIS BOOKApplications of Supercritical Fluids in Industrial Analysis

The continued search for rapid, efficient and cost-effective means of analytical measurement has introduced supercritical fluids into the field of analytical chemistry. Two areas are common: supercritical fluid chroma tography and supercritical fluid extraction. Both seek to exploit the unique properties of a gas at temperatures and pressures above the critical point. The most common supercritical fluid is carbon dioxide, employed because of its low critical temperature (31 °C), inertness, purity, non-toxicity and cheapness. Alternative supercritical fluids are also used and

Multidimensional Chromatography

Multidimensional Chromatography
  • Author : Hernan J. Cortes
  • Publisher : CRC Press
  • Release Date : 2020-07-24
  • ISBN : 9781000104226
GET THIS BOOKMultidimensional Chromatography

This book summarizes all the important aspects of multidimensional separations, providing information on gas, liquid and thin-layer chromatography, as well as the techniques and applications of supercritical fluid chromatography in the multidimensional mode.

The Application of Green Solvents in Separation Processes

The Application of Green Solvents in Separation Processes
  • Author : Francisco Pena-Pereira,Marek Tobiszewski
  • Publisher : Elsevier
  • Release Date : 2017-02-28
  • ISBN : 9780128054437
GET THIS BOOKThe Application of Green Solvents in Separation Processes

The Application of Green Solvents in Separation Processes features a logical progression of a wide range of topics and methods, beginning with an overview of green solvents, covering everything from water and organic solvents, to ionic liquids, switchable solvents, eutectic mixtures, supercritical fluids, gas-expanded solvents, and more. In addition, the book outlines green extraction techniques, such as green membrane extraction, ultrasound-assisted extraction, and surfactant-mediated extraction techniques. Green sampling and sample preparation techniques are then explored, followed by green analytical separations,

Handbook of Food Analysis Instruments

Handbook of Food Analysis Instruments
  • Author : Semih Otles
  • Publisher : CRC Press
  • Release Date : 2016-04-19
  • ISBN : 9781420045673
GET THIS BOOKHandbook of Food Analysis Instruments

Explore the Pros and Cons of Food Analysis InstrumentsThe identification, speciation, and determination of components, additives, and contaminants in raw materials and products will always be a critical task in food processing and manufacturing. With contributions from leading scientists, many of whom actually developed or refined each technique or